u/ProtectionKey7505

▲ 8 r/LSA

LSA Purification Procedure?

So I have a fairly decent background in chemistry, and I came up w/ this procedure. I'm curious if anyone has tried it or anything similar to get (what should be) a fairly decent yield beyond most purification I've seen. (Unfortunately, I don't have most of the equipment needed, so I can't perform it)

My whole idea is that if you can do a acid/base extraction while keeping pH around an 8 to get the LSA in freebase form than add a nonpolar solvent, you should get a lot of LSA w/o plant matter. Once you pull a vacuum (w/ mostly a noble gas present), evap most the solvent, then from there convert it into a salt, I imagine you should have fairly decent (and storable) LSA.

I've not seen any posts relating to extraction/purification past CWE, but if I'm deadwrong and there's posts more directed past CWE please direct me to it. 🙏

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u/ProtectionKey7505 — 4 days ago